Learn · Organic Chemistry

Tosylates and Mesylates

Converting the awful –OH leaving group into an excellent sulfonate ester — without touching the C–O carbon.

Quick answer –OH is a terrible leaving group, so activate it: TsCl/pyridine gives a tosylate (–OTs), MsCl/Et3N a mesylate (–OMs). This happens at oxygen (configuration retained); the later SN2 then inverts the carbon.

The alcohol is the most common functional group in organic chemistry — and one of the worst leaving groups. Attach its oxygen to a sulfonyl group and that same carbon suddenly rivals bromide and iodide.

Ethanol — –OH won't leave
Ethyl tosylate (–OTs) — leaves easily
Ethyl mesylate (–OMs) — leaves easily

Same C–O carbon, three fates: as an alcohol it is inert, but as a sulfonate ester it is primed to react. Structures drawn live.

1. The Hydroxyl Group Must Be Activated Because Hydroxide Is a Terrible Leaving Group

Hydroxide is a strong base (pKa of water ≈ 15.7), so it clings to carbon and R–OH won't do a plain SN2.

Hydroxide — strong base, bad LG
Ethoxide — also a strong base

2. TsCl Gives a Tosylate and MsCl Gives a Mesylate — the C–O Bond Is Never Touched

The alcohol oxygen attacks sulfur and chloride leaves: TsCl/pyridine gives –OTs, MsCl/Et3N gives –OMs, all without breaking the C–O bond.

Ethanol → ethyl tosylate. Swap TsCl/pyridine for MsCl/Et3N to get the mesylate instead.

3. A Sulfonate Is a Weak Base, So It Is an Excellent Leaving Group

Sulfonic acids are strong (TsOH pKa ≈ −2.8), so their conjugate bases are weak, delocalized, and leave readily: –OTf > –OMs ≈ –OTs > I > Br ≫ –OH.

Bromoethane (Br)
Ethyl iodide (I)
Ethyl tosylate (–OTs)
Ethyl triflate (–OTf) — best of all

Leaving-group comparison: sulfonate esters sit right alongside — or above — the good alkyl halides.

4. Once Made, R–OTs Does SN2, SN1, or E2 Just Like an Alkyl Halide

A tosylate is a "super halide" that plugs into any substitution or elimination — azide gives an alkyl azide, cyanide extends the chain to a nitrile.

Ethyl tosylate + azide → ethyl azide by a clean SN2 displacement of OTs.

Cyanide displaces the tosylate to build a new C–C bond, giving a nitrile (propanenitrile).

5. Making the Tosylate Retains Configuration; the SN2 Then Inverts It

Sulfonylation never touches the stereocenter (retention), while the following backside SN2 inverts it — so the overall sequence gives defined net inversion.

(S)-2-butanol → its tosylate with retention — the C–O carbon is never touched.

A single stereocenter alcohol — configuration set.
TsCl/pyridine: sulfonylation at oxygen keeps the carbon's configuration (retention).
A nucleophile then does SN2 from the backside — inversion — expelling OTs.

6. Summary

–OH is a bad leaving group · TsCl/pyridine → –OTs, MsCl/Et3N → –OMs, –OTf most reactive · sulfonates are weak bases from strong acids · activation retains configuration · the SN2 then inverts · net: alcohol → tosylate → substitution with defined inversion.

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Direct SN2 would require expelling hydroxide (OH), a strong base and a terrible leaving group, so nothing happens. Converting the alcohol to ethyl tosylate with TsCl/pyridine replaces –OH with –OTs, the weak, stable conjugate base of a strong sulfonic acid. Now cyanide displaces the sulfonate easily to give the nitrile — the leaving group changed, the carbon did not.

A leaving group departs as a base, and weaker bases leave better. OH is the conjugate base of water (pKa ≈ 15.7) — a strong base. OTs is the conjugate base of p-toluenesulfonic acid (pKa ≈ −2.8), a strong acid — so its conjugate base is very weak and stabilized by delocalization over three oxygens. Weak base = excellent leaving group.

Tosylate formation happens only at oxygen — the C–O bond is never broken — so configuration is retained; the tosylate has the same spatial arrangement as the alcohol. The subsequent SN2 is a backside attack, which inverts the stereocenter. Net over the two steps: inversion, but by a fully predictable path.

–OTf > –OMs ≈ –OTs > I > Br ≫ –OH. The three sulfonates are all excellent because they come from strong acids (triflic > methanesulfonic ≈ toluenesulfonic). Reagents: TsCl with pyridine makes the tosylate; MsCl with Et3N makes the mesylate.

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